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To that, distillers add other grains like corn, barley, or wheat to make the whiskey sweeter, spicier, and more rounded. Also, it shouldn’t be bottled at less than 40% ABV . From there, the grains are heated in peat smoke, mashed, fermented, distilled, and then left to mature in oak barrels.
If you want to move one step further, you can manufacture alcohol based fuel for home use by obtaining a Federal Fuel Alcohol permit – which is inexpensive, easy to obtain and maintain. It might help to remember that in countries with an ‘e’ in the name, the correct spelling is “whiskey”, with an ‘e’. In countries without an ‘e’ in the name, the correct spelling is “whisky”, without an ‘e’.
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But there is one last component to the whiskey making process, and that’s one that you can absolutely do legally in your own home. Use a proof and tralle hydrometer to test the ABV of your moonshine. At this point, you have moonshine — high ABV whiskey. In order to get it resembling something like you'd find at the store, you need to age the whiskey and dilute it down to 40% - 50% ABV.

Proofing is the process of adding water to your whiskey to reach the desired alcohol by volume level for drinking. This is generally between 40% and 50% alcohol by volume. Make sure to cur your whiskey with clean spring water with no iron present. Alcohol content is measured using a spirit hydrometer and graduated cylinder. It is a good idea to use malted grains when making whiskey because they contain a higher sugar content than grains which have not been malted.
How to Distill Whiskey Yourself
Its perfectly legal to own a still, and you can even use it, as long as youre not making alcohol so, you can make essential oils without a permit, or perfume, or distilled water. During the distillation, the earliest liquid fermented should not be consumed. Remove the first 1/4 cup of heads that comes out of the condenser tube. The heads contain a high concentration of methanol which is poisonous. The first step in making mash is heating 5-gallon water to roughly 165 °F in a mash pot. Immediately pour the maize into the water and stir for 3-5 minutes.
Even if you cleaned your whiskey moonshine still after your last run and let it sit for a while, it is still recommended to clean it before transferring your whiskey mash water. This is especially the case on copper stills that are starting to show a salt buildup. If you have tocarbon-filter a whiskey to make it taste better, youve done something horriblywrong and might as well throw it out.
Difference Between Scotch and Whiskey
Another option that you have is the ability to add flavors beyond just the charred oak. The first benefit is that this is a very compact process. There’s no need for a lot of space or a huge investment in equipment, it can be as simple as popping the cork on a bottle of whiskey and dropping a stick of wood inside. As seen in my photo above, you can do it in a mason jar if that’s what you have handy. The same thing is happening in the whiskey world today, with mass produced whiskey from places like MGP in Indiana going to smaller distilleries that all put their own twist on the product. Aging the whiskey in unique materials or unique climates, and all of them getting different results.
Your skill as a home bourbon distiller will come into play, because you need to gauge the beginning and end of the hearts portion of the distillation run. You can do this by tasting not swallowing a small portion of your distillate to ensure that it doesn’t taste like solvents. These are the first vapors to boil off during distillation during heating, and contain methanol and other undesirables. Foreshots account for 5 percent of your total distillate, and should always be discarded and never consumed, as it can make you blind.
Once the final product is bottled, the taste will no longer improve. To make whisky, first place a burlap sack full of corn kernels in a bucket of warm water. Let the corn soak for 10 days, then remove any sprouted ends from the kernels and crush them with a rolling pin. Once they’re fully mashed, put the kernels in a bucket of boiling water and let the container cool. When the solution reaches 86 °F, add yeast to the mash and pitch it for 5 minutes. Then, cover the bucket with a lid outfitted with an airlock and let the mash ferment for up to 10 days.

That trend continues to this very day – whiskey taxes are here to stay, and so too the restrictions on producing moonshine at home. Ironically, the origin of the Federal restrictions against moonshine without licenses date back to the period shortly after the ratification of the US Constitution and the Bill of Rights . The newly formed republic had substantial debts (to the tune of approximately $80 million) from the Revolutionary War and subsequent expenses. Desperate for revenues, President Washington decided to levy an excise tax on whiskey.
"Corn would probably yield the most sugar, and that's what we're after. It will probably make things 'easier,' but that's a relative term here," Katz said. But corn is likely the least expensive grain to buy in bulk, and probably the easiest grain to work with on a small scale. You would need about 10 pounds to expect a reasonable amount of volume, which should translate to about 5 gallons of final product. You will be charged with a felony if you illegally make distilled spirits at your own home.
However, you must secure the necessary permits and license to distill. As the strained mash boils at 80 degrees Celsius, the alcohol evaporates. The alcohol will travel through a condenser and return to its liquid form.
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